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Beilstein J. Org. Chem. 2017, 13, 2486–2501, doi:10.3762/bjoc.13.246
Graphical Abstract
Scheme 1: Some previously reported iodine(III) dichlorides relevant to this work.
Scheme 2: Syntheses of fluorous compounds of the formula RfnCH2X.
Scheme 3: Syntheses of fluorous compounds of the formula CF3CF2CF2O(CF(CF3)CF2O)xCF(CF3)CH2X'.
Scheme 4: Attempted syntheses of aliphatic fluorous iodine(III) dichlorides RfnICl2.
Scheme 5: Syntheses of aromatic fluorous compounds with one perfluoroalkyl group.
Scheme 6: Syntheses of aromatic fluorous compounds with two perfluoroalkyl groups.
Figure 1: Partial 1H NMR spectra (sp2 CH, 500 MHz, CDCl3) relating to the reaction of 1,3,5-(Rf6)2C6H3I and Cl...
Figure 2: Two views of the molecular structure of 1,3,5-(Rf6)2C6H3I with thermal ellipsoids at the 50% probab...
Figure 3: Ball-and-stick and space filling representations of the unit cell of 1,3,5-(Rf6)2C6H3I.
Figure 4: Free energies of chlorination of relevant aryl and alkyl iodides to the corresponding iodine(III) d...
Scheme 7: Other relevant fluorous compounds and reactions.
Figure 5: Views of the helical motif of the perfluorohexyl segments in crystalline 1,3,5-(Rf6)2C6H3I (left) a...
Beilstein J. Org. Chem. 2014, 10, 3031–3037, doi:10.3762/bjoc.10.321
Scheme 1: Synthesis of polycyclic fused triazoles.
Scheme 2: Synthesis of fused triazole 4a using phenylacetylene.
Scheme 3: Synthesis of 1a, 1b and 1c.
Scheme 4: Synthesis of fused polycyclic triazole analogs 4.
Figure 1: ORTEP diagram of 4f (CCDC 979471).
Scheme 5: Proposed mechanism for the formation of 4.